Ultrasonic probing of the elastic properties of PMMA bead packings and their rearrangement during pressure sintering

Ultrasound transmission in PMMA spherical bead packings is investigated during the sintering process under stress. Velocity and amplitude measurements of coherent longitudinal waves are performed to monitor the evolution of the elastic properties of the solid frame from noncohesive packing to sintered granular material. Comparison between the experimental velocity data and the prediction by a contact model [Digby, J. Appl. Mech. 48, 803, (1981)] reveals the crucial role of the bonding effect on the mechanical behavior of granular compacts. By using the correlation technique of acoustic speckles, we also observe the important rearrangements in granular packings before the onset of sintering.Comment: to be published in Powder Technology, 8 pages, 8 figure

Sound pulse broadening in stressed granular media

International audienceThe pulse broadening and decay of coherent sound waves propagating in disordered granular media are investigated. We find that the pulse width of these compressional waves is broadened when the disorder is increased by mixing the beads made of different materials. To identify the responsible mechanism for the pulse broadening, we also perform the acoustic attenuation measurement by spectral analysis and the numerical simulation of pulsed sound wave propagation along one-dimensional disordered elastic chains. The qualitative agreement between experiment and simulation reveals a dominant mechanism by scattering attenuation at the high-frequency range, which is consistent with theoretical models of sound wave scattering in strongly random media via a correlation length

Time reversal of ultrasound in granular media

Time reversal (TR) focusing of ultrasound in granular packings is experimentally investigated. Pulsed elastic waves transmitted from a compressional or shear transducer source are measured by a TR mirror, reversed in time and back-propagated. We find that TR of ballistic coherent waves onto the source position is very robust regardless driving amplitude but provides poor spatial resolution. By contrast, the multiply scattered coda waves offer a finer TR focusing at small amplitude by a lens effect. However, at large amplitude, these TR focusing signals decrease significantly due to the vibration-induced rearrangement of the contact networks, leading to the breakdown of TR invariance. Our observations reveal that granular acoustics is in between particle motion and wave propagation in terms of sensitivity to perturbations. These laboratory experiments are supported by numerical simulations of elastic wave propagation in disordered 2D percolation networks of masses and springs, and should be helpful for source location problems in natural processes.Comment: 15 pages, 6 figure

Dynamic induced softening in frictional granular material investigated by DEM simulation

A granular system composed of frictional glass beads is simulated using the Discrete Element Method. The inter-grain forces are based on the Hertz contact law in the normal direction with frictional tangential force. The damping due to collision is also accounted for. Systems are loaded at various stresses and their quasi-static elastic moduli are characterized. Each system is subjected to an extensive dynamic testing protocol by measuring the resonant response to a broad range of AC drive amplitudes and frequencies via a set of diagnostic strains. The system, linear at small AC drive amplitudes has resonance frequencies that shift downward (i.e., modulus softening) with increased AC drive amplitude. Detailed testing shows that the slipping contact ratio does not contribute significantly to this dynamic modulus softening, but the coordination number is strongly correlated to this reduction. This suggests that the softening arises from the extended structural change via break and remake of contacts during the rearrangement of bead positions driven by the AC amplitude.Comment: acoustics, nonlinearity, granular medi

Acoustic Monitoring of Inelastic Compaction in Porous Granular Materials

We study the transition from cohesive to noncohesive granular states of synthetic rocks under oedometric loading, combining simultaneous measurements of ultrasound velocity and acoustic emissions. Our samples are agglomerates made of glass beads bonded with a few percent of cement, either ductile or brittle. These cemented granular samples exhibit an inelastic compaction beyond certain axial stresses likely due to the formation of compaction bands, which is accompanied by a significant decrease of compressional wave velocity. Upon subsequent cyclic unloading and reloading with constant consolidation stress, we found the mechanical and acoustic responses similar to those in noncohesive granular materials, which can be interpreted within the effective medium theory based on the Digby bonding model. Moreover, this model allows P-wave velocity measured at vanishing pressure to be interpreted as an indicator of the debonding on the scale of grain contact. During the inelastic compaction, stick-slip like stress drops were observed in brittle cement-bonded granular samples accompanied by the instantaneous decrease of the P-wave velocity and acoustic emissions which display an Omori-like law for foreshocks, i.e., precursors. By contrast, mechanical responses of ductile cement-bonded granular samples are smooth (without visible stick-slip like stress drops) and mostly aseismic. By applying a cyclic loading and unloading with increasing consolidation stress, we observed a Kaiser-like memory effect in the brittle cement-bonded sample in the weakly damaged state which tends to disappear when the bonds are mostly broken in the non-cohesive granular state after large-amplitude loading. Our study shows that the macroscopic ductile and brittle behavior of cemented granular media is controlled by the local processes on the scale of the bonds between grains.Comment: 22 pages, 15 figure